We learned from lab lecture that Clove Oil is made up of 85% Eugenol, 10% Acetyl Eugenol, and 5% Beta Caryophyllene. Starting this experiment, we knew that the extraction was going to form varies layers due to the density differences. When placing three different substances, we saw that two layers formed because the Clove Oil is soluble in MTBE, but not in water. In order, to get the organic layer we used separatory funnel to take out the excess substances and leave the oil layer. Then we transferred to a beaker and dried with Magnesium Sulfate. Lastly, we filtered the liquid using funnel; we placed the liquid to boil, let it cool to room temperature. The purpose of drying and evaporation is to help us with the Gas Chromatography analysis of the product.
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... peak between 125-200 second. This increased may have occurred due to not having enough amount of Beta-Caryophyllene to be read in the sample. Overall, this experiment was similar to the accepted values, expect for the minor errors that may have occurred.
Indeed, I accomplished my objectives in this experiment of isolating the components in clove oil, Eugenol, and Beta-Caryophyllene. I thoroughly liked this experiment because I learned the techniques to extract and obtain products. Also, helped me to understand why chemical properties are important in solubility. This is relatable to what I learned in class about solubility properties, doing this experiment hands-on taught me the concept of density and solubility. Additionally, understanding this concept portrayed how compounds and solvents behave when mixed together, which was the purpose of this lab.
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