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Explain titration essay
Titration practical writeup
Pratical for titration
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To undertake titration and colorimetry to determine the concentration of solutions
By carrying out titrations and colorimetry, the aim of this investigations was to use these methods such that the concentrations of different solutions used can be identified, and to help find the concentration of the unknown solution that were given. Using Titration and colorimetry the concentrations of different solutions in general can be determined and this helps to identify solutions with unknown concentrations. In this assignment I was asked to carry out two different scientific techniques and find the concentration of different solutions.
Titration of sodium carbonate and sodium hydroxide
I was asked to find the concentration of a solution of sodium
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The equipment I had to calibrate was a pipette, top pan balance and a pH meter. Calibration is a marking a scale on a measuring instrument. This involves establishing the relationship between indications of a measuring instrument and standard or reference quantity values, which must be applied. Calibration is important when conducting an experiment. For example, broken or wrongly calibrated pH meters can give incorrect results, making the results useless. In a research laboratory this could lead to wrong conclusions, wasted time and wasted …show more content…
Its concentration is usually given in mol dm-3. A standard solution is created using a powdered form of the substance and dissolving it in distilled water to make a solution where you know the concentration. When making up a standard solution it is important that the correct mass of substance is accurately measured. It is also important that all of it is transferred to the volumetric flask used to make up the solution. The following procedure will make sure that this happens. Using these solutions will contain accurate concentrations of a chemical component, they will increase confidence regarding the determination of substances with unknown concentrations.
Colorimeter to determine the concentration of two unknown solutions
A colorimeter is a device used to test the concentration of a solution by measuring its absorbance of a specific wavelength of light. It can be used for coloured solutions of different concentrations. Before it can be used I had to calibrate the colorimeter. To do this I had to calibrate a colorimeter a cuvette filled with distilled water is placed into the colorimeter, the colorimeter in theory should then give a reading of the absorbance level being 0, this is because the water used in the calibration process is distilled and therefore should give a reading of 0, if not then it shows the equipment being used the experiment is either faulty or inaccurate. As all the light will pass
Then titrate with the sodium thiosulfate solution as in the standardization procedure, adding 6 drops of starch indicator near the end of the titration. Record the volume of thiosulfate solution used in the titration. Make a duplicate
We were then to make a base solution of 0.7 M NaOH. In order to standardize
A low absorbency would have a low color change so would be clear or slightly clear by the end of the trails and a high absorbency would have a strong red color by the end of the experiment.
...s strength in the experiment rather than a limitation which future studies should also monitor.
We were not given any instructions either to shake or not to shake the test tubes with the coloured solutions before inserting them in the spectrophotometer to read the absorbance. By shaking each test tube a certain number of times before putting it in the spectrophotometer could have improved the accuracy of the of absorbance of the solutions.
The materials used in the previous were cleaned and dried. 10ml of CV was obtained along with 10ml of sodium hydroxide. These solutions were separately diluted to 50ml. A stopwatch was set up to record in 30second increments and the Spectrophotometer prepped for the cuvette. The following steps were done within 30seconds. The two solutions (CV and sodium hydroxide) were mixed in a large beaker. A pipette was used to deliver the solution into a test tube serving as the cuvette. The absorbance was recorded every 30second until 15minutes had passed and entered into a spreadsheet. All used materials were cleaned for the next trial.
Once the mixture had been completely dissolved, the solution was transferred to a separatory funnel. The solution was then extracted twice using 5.0 mL of 1 M
= = = Electronic Balance (accurate to 2 decimal places) Goggles Spatula Distilled Water ( 250cm3) Anhydrous Sodium Carbonate (2.65g) Beaker - 250cm3 Stirring Rod Petri Dish Pipette Volumetric flask Requirements for the titration experiment: - =
Determining the Concentration Of Limewater Solution Aim: The aim of this experiment is it to find out the concentration of Limewater by performing a titration with hydrochloric acid which has concentration exactly 2.00M.. What is required for me is that I have to design my own experiment and chose the right and appropriate apparatus and equipment. I will be provided with 250cm3 of limewater, which has been made to which contains approximately 1g/dm3 of calcium Hydroxide. This hypothesis from www.studentcentral.co.uk We were also give Hydrochloric acid (HCl) with a concentration of 2.00 mol/dm3 normal laboratory apparatus was also given and so was an indicator.
By doing this experiment, I can know the physical and chemical properties of these samples. After I get my results about the physical and chemical properties of these samples, I can compare my results with the information given by the past student and identify the 5 unknown samples, finding out which sample is which substance. Hypothesis = ==
Using a concentration of.1 NaOH. We had the largest NaOH volume before the largest pH increase at 6.38ml. For the largest NaOH volume after the largest pH increase we used 6.73ml of base. The volume of NaOH used at the equivalence point, pH 7, was 6.575ml. The moles of NaOH used at this point were.0006575mols.
If someone needed a test that was more accurate and detailed to analysis how accurately they can see perceive colors, they would need to take a quantitative color blind test. The most popular test to use is the Farnsworth-Munsell 100 hue test. The test consists of four trays containing many small disks of varying hues. Each tray has a color reference disk at one end. The person being tested must arrange the other disks within the tray to create a continuum of gradually changing hue.
2. Photometer; after the chosen range of wavelength of light passes through the solution of a sample in cuvette, the photometer detects the amount of photons that is absorbed and then sends a
A refractometer is an optical device that is used to measure the optical density or refractive index of a substance. Refractive index is a dimensionless number that describes how light, or any other radiation is bent as it moves through a medium. It is the ratio of light’s velocity in a vacuum (n=1) to its velocity in the sample. The greater the increase in optical density or refractive index, the greater the speed of light is reduced in a solid, gas or solution. A refractometer measures the refractive index of liquids, gases and translucent solids like gemstones. There are four main types of refractometers: traditional handheld refractometers, digital handheld refractometers, laboratory or Abbe refractometers, and inline process refractometers, (Wikipedia - Refractometers). Scientists often use refractometers to measure the refractive index when studying the physical properties of different solids and liquids. Bench and handheld refractometers are usually used for more practical purposes, for example to measure the concentration of a dissolved substance.
For this experiment we used titration to standardize the exact concentration of NaOH. Titration is the process of carefully adding one solution from a buret to another substance in a flask until all of the substance in the flask has reacted. Standardizing is the process of determining a solutions concentration. When a solution has been standardized it is referred to as a standard solution. To know when a solution is at its end point an indicator is added to acidic solution. An indicator is an organic dye that is added to an acidic solution. The indicator is one color is in the acidic solution and another color in the basic solutions. An end point occurs when the organic dye changes colors to indicate that the reaction is over (Lab Guide pg. 141).