Abstract The purpose for this lab was to use aluminum from a soda can to form a chemical compound known as hydrated potassium aluminum sulfate. In the lab aluminum waste were dissolved in KOH or potassium sulfide to form a complex alum. The solution was then filtered through gravity filtration to remove any solid material. 25 mLs of sulfuric acid was then added while gently boiling the solution resulting in crystals forming after cooling in an ice bath. The product was then collected and filter through vacuum filtration. Lastly, crystals were collected and weighed on a scale. Introduction Aluminum is the third most abundant element and most abundant metal in the Earth’s crust. Aluminum is never found in the free element state in nature. It …show more content…
Al to Al(OH)4 – (aq). Cut and Measure approximately one gram of aluminum off the side of a soda can. Take a piece of stainless steel scouring pad to remove the coating from both sides of the aluminum. Cut the Aluminum into smaller pieces to increase the surface area so the rate of the chemical reaction can increase and dissolve more quickly. Reweigh the aluminum to determine its exact mass. In a hood, add the aluminum to a 400mL beaker containing 50mLs of KOH potassium hydroxide. Allow the solution to sit until all of the aluminum has dissolved. This process could take up to 20 minutes. You may also need to use a low heat setting on a hot plate. During the reaction, the product will turn a dark grey color. The reaction is complete once all of the aluminum has dissolved and hydrogen gas ceases to evolve. After the aluminum has dissolved use gravity filtration to remove all solids from the solution, collect the solution into a 250 mL Erlenmeyer …show more content…
The experiment was not a success, there was percent yield of 1,423%. With a percent yield that is relatively high at 1,423% did not conclude a successful experiment, because impurities added to the mass of the actual product. There were many errors in this lab due to the product being transferred on numerous occasions as well, as spillage and splattering of the solution. Overall, learning how to take one product and chemically create something else as well as how working with others effectively turned out to be a
2-ethyl-1,3-hexanediol. The molecular weight of this compound is 146.2g/mol. It is converted into 2-ethyl-1-hydroxyhexan-3-one. This compounds molecular weight is 144.2g/mol. This gives a theoretical yield of .63 grams. My actual yield was .42 grams. Therefore, my percent yield was 67%. This was one of my highest yields yet. I felt that this was a good yield because part of this experiment is an equilibrium reaction. Hypochlorite must be used in excess to push the reaction to the right. Also, there were better ways to do this experiment where higher yields could have been produced. For example PCC could have been used. However, because of its toxic properties, its use is restricted. The purpose of this experiment was to determine which of the 3 compounds was formed from the starting material. The third compound was the oxidation of both alcohols. This could not have been my product because of the results of my IR. I had a broad large absorption is the range of 3200 to 3500 wavenumbers. This indicates the presence of an alcohol. If my compound had been fully oxidized then there would be no such alcohol present. Also, because of my IR, I know that my compound was one of the other 2 compounds because of the strong sharp absorption at 1705 wavenumbers. This indicates the presence of a carbonyl. Also, my 2,4-DNP test was positive. Therefore I had to prove which of the two compounds my final product was. The first was the oxidation of the primary alcohol, forming an aldehyde and a secondary alcohol. This could not have been my product because the Tollen’s test. My test was negative indicating no such aldehyde. Also, the textbook states that aldehydes show 2 characteristic absorption’s in the range of 2720-2820 wavenumbers. No such absorption’s were present in my sample. Therefore my final product was the oxidation of the secondary alcohol. My final product had a primary alcohol and a secondary ketone
The sand is If the water with Alka-Seltzer tablets is stirred during the reaction, then the rates of reactions will increase because the particles will be forced to make contact with each other and... ... middle of paper ... ...results anomalies because they are the outcome of dissociation of calcium and magnesium ions,. Evaluation: What is the difference between My results were very reliable, because by looking at my graphs I can see a trend that relates to my scientific background. It is also evident that I have obtained a reliable set of results when I see that.
Firstly, an amount of 40.90 g of NaCl was weighed using electronic balance (Adventurer™, Ohaus) and later was placed in a 500 ml beaker. Then, 6.05 g of Tris base, followed by 10.00 g of CTAB and 3.70 g of EDTA were added into the beaker. After that, 400 ml of sterilized distilled water, sdH2O was poured into the beaker to dissolve the substances. Then, the solution was stirred using the magnetic stirrer until the solution become crystal clear for about 3 hours on a hotplate stirrer (Lab Tech® LMS-1003). After the solution become clear, it was cool down to room temperature. Later, the solution was poured into 500 ml sterilized bottle. The bottle then was fully wrapped with aluminium foil to avoid from light. Next, 1 mL of 2-mercaptoethanol-β-mercapto was added into fully covered bottle. Lastly, the volume of the solution in the bottle was added with sdH2O until it reaches 500 ml. The bottle was labelled accordingly and was stored on chemical working bench.
... got very different results, however they had carried out the experiment in slightly different ways, making it difficult to compare results.
Calcium is the 20th element of the periodic table. It is a metallic element that is greyish-silver in colour and has the atomic symbol of Ca. It is a group 2 alkaline earth metal and is the 5th most abundant element by mass in earth’s crust. It is also reactive with water and is relatively soft. It is an essential element for organisms, and is major material that is used in the materialisation of teeth, bone and shells. It is also the most abundant metal located within animals.
I did accomplish the purpose of the lab. First, I determined the percentage of water in alum hydrate, and the percentage of water in an unknown hydrate. The results are reasonable because they are close to the example results. Second, I calculated the water of crystallization of an unknown hydrate. Furthermore, I developed the laboratory skills for analyzing a hydrate.
Aluminium is present in the earth's crust in huge amount, mainly in the form of insoluble aluminium silicates. It is scarce in the human body which contain only 30-50 mg of that metal. This is due to the insolubility of aluminium, the presence of a barrier in the gastro-intestinal tract to soluble forms of aluminium, and the ability of the kidneys to excrete aluminium effectively in healthy people.
9. Get your stopwatch ready and drop the Alka-Seltzer tablet at the same time you started the timer. 10. When it finishes dissolving (you can see through the water and there is no more fizzing.) stop the timer and record the results. 11.
The conical vial was placed in a small beaker and allowed to cool to room temperature. The mixture was Cooled thoroughly in an ice bath for 15-20 minutes and crystals collected by vacuum filtration on a Hirsch funnel. The vial was rinsed with about 5 mL of ice water and transferred into to the Hirsch funnel and again washed with two additional 5mL portions of ice water. Crystals were dried for 5-10 minutes by allowing air to be drawn through them while they remained on the Hirsch funnel. The product was transferred to a watch glass plate and allow the crystals to dry in air. Crude acetaminophen product was weighed and set aside a small sample for a melting point determination and a color comparison after the next step. Calculation of the percentage yield of crude acetaminophen (MW = 151.2). was done and recorded in the lab notebook.
In a 100ml beaker place 50mls of water, measure the temperature of the water and record this initial temperature onto a table. Set the timer and add one teaspoon of Ammonium Nitrate to the water, stir this continuously until the Ammonium Nitrate has dissolved.
== Refer to, Chemistry Lab #1 – What’s the substance? However, I changed some of procedures during my experiment, here is the changes I made in this experiment: * I only used the toothpick to place a small amount of each sample on a separate piece of paper, instead of the spatula.
There is also the potential of human error within this experiment for example finding the meniscus is important to get an accurate amount using the graduated pipettes and burettes. There is a possibility that at one point in the experiment a chemical was measured inaccurately affecting the results. To resolve this, the experiment should have been repeated three times.
Aluminum is number thirteen on the periodic table and it’s atomic weight is twenty seven. The melting point of aluminum is 660.2 degrees Celsius. The density of Aluminum is 2.7 grams per cubic centimeter. In nature, aluminum cannot be found uncombined.
Aluminum is an element in the boron group with a symbol of Al, and an atomic number of 13. Aluminum is a very soft metal when pure but becomes strong and hard when alloyed, a malleable metal with a silvery gray color. Aluminum is a very reactive element so it is found in nature combined with other elements. Aluminum resists corrosion by the formation of a self-protecting oxide coating. Aluminum is the third most abundant element in the Earth’s crust, following oxygen and silicon. It makes up approximately 8% by weight of the Earth’s surface. Although this is evident, it is also apparent that aluminum is never found by itself in nature. All of the earth’s aluminum has combined with other elements to form compounds and in order to create new aluminum products; it has to be taken out of that specific compound. Aluminum does not rust like other elements, therefore it always remains strong and shiny, which means reused aluminum is almost identical to a brand new piece of metal. An electrochemical process creates aluminum. An electrochemical process is “the direct process end use in which electricity is used to cause a chemical transformation” ( E.I.A. Government). Major uses of electrochemical processes occur in the aluminum industry in which alumina is reduced to molten aluminum metal and oxygen, where than the aluminum can be used into making several different materials. Electrochemical processes, although very useful, can have serious environmental consequences. To help reduce the consequences that the production of aluminum creates, the idea of aluminum recycling comes into play.