Determining the Empirical Formula of Magnesium Oxide

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Determining the Empirical Formula of Magnesium Oxide

INTRODUCTION:

The empirical formula is the simplest and lowest whole number ratio of

the different atoms in a sample of compound. To work out the empirical

formula, the value of moles of the different atoms in a compound is

needed. Mole is just simply a unit used to measure the amount of

atoms, just like how the unit "dozen" is used to measure things such

as eggs. One mole is 6×10^23 atoms and this number is called the

Avogadro number. The mole can be also defined as the number of atoms

in exactly 12g of Carbon.

In this experiment, the magnesium will be heated and this magnesium

will react with the oxygen in the air to form magnesium Oxide.

DIAGRAM:

METHOD:

1. An empty crucible and its lid were weighed on an electrical

balance. The mass of the crucible and its lid were recorded.

2. The surface of the magnesium ribbon was scraped with emery paper to

remove any magnesium oxide on the surface.

3. The magnesium was coiled and placed in the crucible. Then the lid

was replaced on the crucible, and the mass of the crucible with lid

containing the magnesium was found. The mass was recorded.

4. The safety goggle was worn. Then apparatus was setup as shown in

the diagram. The magnesium was first heated with a small blue flame

and after a several minutes with a roaring flame.

5. Every few minutes, the lid of the crucible was lifted carefully

with a tong to see if the magnesium had started to burn and also to

left some air enter the crucible to make the experiment more

efficient.

6. When the magnesium had completely reacted, the crucible was heated

stron...

... middle of paper ...

...al possible source of error is that some white

fume magnesium oxide escaped from the crucible. This error can be

prevented by performing the experiment in a fume cupboard. The most

significant source of error is that some magnesium possibly reacted

with Nitrogen in the air to form Magnesium Nitride. Since 78% of air

is made up of Nitrogen, it is highly possible that some Magnesium

reacted with the Nitrogen. This made the mass of oxygen that reacted

with the magnesium low, which made the mole of magnesium higher than

the accepted value. This error can be prevented by burning the

magnesium in pure oxygen, not air; although, this is very difficult to

do in reality. One way the experiment can be improved is to perform

the experiment several times and record the average result so that a

more accurate result can be obtained.

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